000 03825nam a22004695i 4500
001 978-3-211-75125-1
003 DE-He213
005 20161121231140.0
007 cr nn 008mamaa
008 100301s2008 au | s |||| 0|eng d
020 _a9783211751251
_9978-3-211-75125-1
024 7 _a10.1007/978-3-211-75125-1
_2doi
050 4 _aTA401-492
072 7 _aTGM
_2bicssc
072 7 _aTEC021000
_2bisacsh
082 0 4 _a620.11
_223
245 1 0 _aMaterials Syntheses
_h[electronic resource] :
_bA Practical Guide /
_cedited by Ulrich Schubert, Nicola Hüsing, Richard M. Laine.
264 1 _aVienna :
_bSpringer Vienna,
_c2008.
300 _aVII, 228 p.
_bonline resource.
336 _atext
_btxt
_2rdacontent
337 _acomputer
_bc
_2rdamedia
338 _aonline resource
_bcr
_2rdacarrier
347 _atext file
_bPDF
_2rda
505 0 _aControlling Size and Morphology of Zeolite L -- Zeolite A and ZK-4 -- Mesostructured Silica Thin Films -- Organically Modified Monolithic Silica Aerogels -- Porous Silica Gel by Acid Leaching of Metakaolin -- Zirconia-Pillared Clays -- Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars -- Birnessite-type Manganese Oxide by Redox Precipitation -- Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices -- Fiberous Carbon from Sepiolite Clay and Propylene -- Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder -- Sonochemically Prepared Molybdenum Sulfide -- Doped Manganites -- Lithium Manganese Oxide Prepared by Flux Methods -- Nanoscale Magnesium Oxide -- Nanostructured Pt-doped Tin Oxide Films -- Organically Functionalized Silica Nanoparticles -- Copper Nanoparticles in Silica -- Copper Nanocrystals -- Assembly of TOPO-Capped Silver Nanoparticles to Multilayered Films -- Colloidal Dispersion of Gold Nanoparticles -- One-dimensional Nanorods and Nanowires -- Monolithic Tin-doped Silica Glass -- Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites -- Polysilsesquicarbodiimide Xerogels -- Polyaniline — A Conducting Polymer -- Allyl- and Hydroxytelechelic Poly(isobutylenes) -- Symmetrically and Unsymmetrically Substituted Phthalocyanines.
520 _aMaterials syntheses are generally more complex than syntheses of inorganic or organic compounds, and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. A number of detailed protocols has been collected, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis. Each contribution provides detailed and unambiguous description of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.
650 0 _aMaterials science.
650 0 _aInorganic chemistry.
650 0 _aNanotechnology.
650 1 4 _aMaterials Science.
650 2 4 _aMaterials Science, general.
650 2 4 _aInorganic Chemistry.
650 2 4 _aNanotechnology.
700 1 _aSchubert, Ulrich.
_eeditor.
700 1 _aHüsing, Nicola.
_eeditor.
700 1 _aLaine, Richard M.
_eeditor.
710 2 _aSpringerLink (Online service)
773 0 _tSpringer eBooks
776 0 8 _iPrinted edition:
_z9783211751244
856 4 0 _uhttp://dx.doi.org/10.1007/978-3-211-75125-1
912 _aZDB-2-CMS
950 _aChemistry and Materials Science (Springer-11644)
999 _c509299
_d509299